Carboxylic acids
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How is benzoic acid commonly produced in the lab?
Benzoic acid is produced by the oxidation of alkylbenzenes, such as toluene, using hot alkaline potassium manganate(VII) (KMnO₄) as the oxidising agent. The alkyl group is oxidised to the carboxyl group.
What products are formed when a carboxylic acid reacts with PCl₃ and heat?
A carboxylic acid reacts with PCl₃ and heat to form an acyl chloride, phosphorus acid (H₃PO₃), and HCl.
Write the balanced equation for the oxidation of methanoic acid (HCOOH) with acidified potassium permanganate (KMnO₄).
2KMnO₄ + 5HCOOH + 3H₂SO₄ → K₂SO₄ + 2MnSO₄ + 5CO₂ + 8H₂O. Methanoic acid is oxidised to carbon dioxide and water.
Describe the reaction of ethanedioic acid (HOOCCOOH) with warm acidified KMnO₄.
Ethanedioic acid is oxidised to carbon dioxide by warm, acidified potassium permanganate (KMnO₄). The purple colour of the KMnO₄ decolourises as MnO₄⁻ is reduced to Mn²⁺.
Explain the relative acidities of carboxylic acids, phenols, and alcohols.
Carboxylic acids are generally more acidic than phenols, which are more acidic than alcohols. This is because the negative charge on the carboxylate ion (RCOO⁻) is delocalised over two oxygen atoms, making it more stable than the phenoxide ion (delocalised over the benzene ring). Alkoxide ions are the least stable.
How does the presence of chlorine substituents affect the acidity of carboxylic acids? Explain why.
Chlorine substituents increase the acidity of carboxylic acids. This is because chlorine is electron-withdrawing, which stabilises the carboxylate anion by dispersing the negative charge, making the acid more likely to donate a proton.
Write the general equation for the reaction of a carboxylic acid with thionyl chloride (SOCl₂).
RCOOH + SOCl₂ → RCOCl + SO₂ + HCl. This reaction produces an acyl chloride, sulfur dioxide, and hydrogen chloride gas.
What is the product formed when ethanoic acid reacts with phosphorus pentachloride (PCl₅)?
The reaction of ethanoic acid (CH₃COOH) with phosphorus pentachloride (PCl₅) forms ethanoyl chloride (CH₃COCl), phosphorus oxychloride (POCl₃), and hydrochloric acid (HCl).
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